15 oct 2012

Equations with indicator variables - part 1


Sometimes it is necessary to merge spectra files from different instruments (standardized or not) to get a bigger data base with more variability, range,…
We would like that all the laboratory values would come from the same lab, but this is not normally the case, and the lab data comes from different labs (probably one for each instrument). In that case we can add some indicator variables to help on this to the software.
Suppose we have 2 spectra files, one from one instrument (1) with lab values from Lab1, and  the other from a different instrument (2) with lab values from Lab2. In this case we create an indicator variable adding “ceros”  for the instrument 1_lab1 spectra:
0
0
0
And “ones” to the instrument2_ lab2 spectra :
1
1
1
In the case of three instruments, three labs, we would need 2 indicator variables:
For instrument 1_lab1:
0          0
0          0         
0          0         
For instrument 2_lab2:
1          0
1          0         
1          0
For instrument 3_lab3:
0          1
0          1         
0          1
In the case of 4 instruments, four labs, we would need 3 indicator variables:
For instrument 1_lab1:
0          0          0
0          0          0
0          0          0
For instrument 2_lab2:
1          0          0
1          0          0
1          0          0
For instrument 3_lab3:
0          1          0
0          1          0
0          1          0
For instrument 4_lab4:
0          0          1
0          0          1
0          0          1
And so on,
Of course we can use this method for only one instrument with lab data from four labs, so in this case it will be:
Instrument 1_lab1, instrument 1_lab2, instrument 1_lab3 and instrument 1_lab4

8 oct 2012

Updating to Win ISI 4.xx (does not recognize the dongle)


When installing Win ISI 4 in a new computer, see first if the software is a full version or an upgrade.
If the software is an upgrade and you install it as a full version, it will not recognize the dongle. By default the installation program choose "Full Version", so it is easy to make this mistake.

7 oct 2012

William Herschell experiment


This is a good link to a page where the experiment of Sir William Herschell (discovering the NIR region) is developed and very well described with cheap materials.
An Example of the Herschel Experiment
















3 oct 2012

Jornada sobre control de procesos con NIR

Hoy día 3 de Octubre, se ha celebrado una jornada para usuarios de equipos NIR, para mostrarles las ventajas de los equipos NIR "on line". Las jornadas se desarrollaron en un hotel centrico de Segovia donde se realizaron unas interesantes ponencias y posteriormente se visito la fábrica de Garese, donde los anfitriones (Lorenzo y Patricia) nos mostraron sus magníficas inslalaciones, y nos comentaron las ventajas que les aporta el control del pienso con un equipo NIR de procesos.
Salieron comentarios interesantes acerca de como tratar la cantidad de datos que se generan, con el fín de obtener el mayor beneficio de este tipo de equipos.

El tomamuestras utilizado para recoger una muestra representativa para analizar por el método de referencia es de Barreal y lo podéis ver en:


1 oct 2012

Getting a representative sample - 01


In the NIR we analyze a small sample, which has to be representative of a huge amount, so it is important to split the first sampling from the truck into another smaller representative sample. This video shows an easy way to do it.
After this, the sample is grinded, homogenized, and placed in a small cup to be analyzed in the instrument.

En los equipos NIR, analizamos partes muy pequeñas que deben de representar a grandes cantidades. Es por tanto importante el cuartear la muestra inicial recogida con un tomamuestras o lanza del camión, para obtener una mas pequeña y representativa, que será molida, homogenizada y añadida a la cubeta para ser analizada.

Agradecimientos a  Emilio de "Cereales La Almarcha".